ID22 - High resolution powder diffraction beamline

Status: open

Disciplines

Chemistry
Physics
Materials and Engineering
Environmental Sciences
Cultural Heritage
Earth and Planetary Sciences
Life Sciences

Techniques

DAFS - Diffraction Anomalous Fine Structure
HR-XRPD - High-Resolution X-ray Powder Diffraction
HT-XRD - High-Temperature X-ray Diffraction
PDF - Pair Distribution Function
WAXS - Wide-angle X-ray Scattering
XRPD - X-ray Powder Diffraction

Energy range

6.0 - 75.0 keV

Beam size

Minimum (H x V) : 0.05 x 0.05 mm²
Maximum (H x V) : 1.0 x 1.0 mm²

Sample environments

Temperature: 4 K to 1800 K
Capillary gas cell (0 - 100 bar)
Flow cell with mass spectrometer

Detectors

13-channel Si 111 multianalyser stage

Dectris Eiger2 X 2M-W CdTe pixel detector.
Perkin Elmer XRD1611.

Technical details

ID22 is the high resolution powder diffraction beamline.

Please see https://doi.org/10.1107/S1600577523004915 ( J. Synchrotron Radiation (2023), 30, 1003-1012) for further details.

Latest publications

View all publications

Coupled structural and electronic transitions in the layered Ni5.7SnSe2 metal

Agnarelli L., Prots Y., Schmidt M., Rosner H., Fitch A., Pelloquin D., Hébert S., Maignan A.,
Chemistry of Materials 38, 4008-4016 (2026)

Ba(PO4)2M5+2O3 mixed metal systems (M = Nb, Ta, W) at the edge between dielectrics and 2D-metals

Al Bacha S., Aréalo-López A.M., Terryn C., Glaum R., Cano A., Mentré O.,
Solid State Sciences 179, 108376-1-108376-8 (2026)

Superlattice phase precipitation in Ti-Fe-Mo-Al alloys

Andersson A.M.L., Mellor R.F.L., Hogg J.M., Cole H.C., Lampronti G.I., Church N.L., Houghton O.S., Jones N.G., Stone H.J.,
Materials Characterization 234, 116139-1-116139-10 (2026)

Additive-specific modulation of non-classical nucleation pathways

Baken A., Fernández-Martínez A., Lanson M., Aretxabaleta X.M., Manzano H., Kellermeier M., Di Michiel M., Van Driessche A.E.S.,
Nature Communications 17, 1925-1-1925-14 (2026)

Short-range structure and reactivity in phosphate-based geopolymers

Bernasconi D., Celikutku C., Bordignon S., Jafri S.F., Maximenko A., Paul G., Bernasconi A., Borfecchia E., Gobetto R., Viani A., Pavese A.,
Materials Chemistry and Physics 358, 132457-1-132457-16 (2026)

Protection efficiency of zinc chromate-based historical primers: A multiscale investigation by electrochemical and spectroscopy methods

Brunet M., Holé C., Balbo A., Faulmann C., Warot-Fonrose B., Monico L., Sciau P.,
Journal of Cultural Heritage 79, 273-284 (2026)

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