Synopsis
Beamline ID27 is a premier X-ray powder and single crystal diffraction station (nanofocus) primarily dedicated to research at extreme pressures and temperatures.
The beamline is currently being upgraded. The webpage will be updated in parallel. Please contact the scientist in charge for the current status.
Status:
open
Disciplines
- Physics
- Earth and Planetary Sciences
- Materials and Engineering
- Chemistry
- Environmental Sciences
- Life Sciences
Applications
- Earth and planetary sciences
- Fundamental physics
- Chemistry
- Materials research
- Biophysics/biochemistry
- Life and biological function under extreme conditions.
Techniques
-
Powder diffraction
-
XRD - X-ray diffraction
-
XRF - X-ray fluorescence
Beam size
- Minimum (H x V) : 300.0
x 250.0
nm²
-
Maximum (H x V) : 2.0
x 2.0
µm²
Sample environments
- Double sided laser heating diamond anvil cell (YAG and CO2; T up to 5000 K)
- Resistively heated diamond anvil cell (T up 1000 K)
- High pressure He flow cryostat (T down to 5 K)
- Paris-Edinburgh cell
- Nano-positioning stage
Detectors
- EIGER2 X CdTe 9M detector
Technical details
Beamline ID27 has been operating since 2006 in replacement of ID30 (an instrument which was mostly dedicated to white beam experimentation). This instrument is fully optimised for monochromatic high-resolution XRD in order to address the most exciting and challenging questions related to science at very high pressures. The beamline can easily accommodate very complex sample environments such as a double-sided laser heating system, Paris-Edinburgh press and HP helium cryostat. Techniques available are powder and single-crystal microdiffraction, and X-ray microfluorescence.
Atomic-spring-like effect in glassy silica-helium composites
Bowron D.T., Keen D.A., Kint M., Weigel C., Rufflé B., Konczewicz L., Contreras S., Coasne B., Garbarino G., Beaudhuin M., Haines J., Rouquette J.,
Journal of Physical Chemistry C 126, 5722-5727 (2022)
Single‐bonded cubic AsN from high‐pressure and high‐temperature chemical reactivity of arsenic and nitrogen
Ceppatelli M., Scelta D., Serrano-Ruiz M., Dziubek K., Morana M., Svitlyk V., Garbarino G., Poreba T., Mezouar M., Peruzzini M., Bini R.,
Angewandte Chemie International Edition 61, e202114191-1-e202114191-9 (2022)
Equilibria between conformational states of the Ras oncogene protein revealed by high pressure crystallography
Girard E., Lopes P., Spoerner M., Dhaussy A.C., Prangé T., Kalbitzer H.R., Colloc'h N.,
Chemical Science 13, 2001-2010 (2022)
The Fe-Si-C system at extreme P-T conditions: A possible core crystallization pathway for reduced planets
Miozzi F., Morard G., Antonangeli D., Baron M.A., Pakhomova A., Clark A.N., Mezouar M., Fiquet G.,
Geochimica et Cosmochimica Acta 322, 129-142 (2022)
Evidence and stability field of fcc superionic water ice using static compression
Weck G., Queyroux J., Ninet S., Datchi F., Mezouar M., Loubeyre P.,
Physical Review Letters 128, 165701-1-165701-6 (2022)
Stability and equation of state of face-centered cubic and hexagonal close packed phases of argon under pressure
Dewaele A., Rosa A.D., Guignot N., Andrault D., Rodrigues J.E.F.S., Garbarino G.,
Scientific Reports 11, 15192-1-15192-12 (2021)