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ID32 - Soft X-ray spectroscopy

Synopsis

X-ray Magnetic Circular Dichroism (XMCD) branch with high field superconducting magnet, variable X-ray spot size at the sample, coupled to a RIXS spectrometer and surface science preparation facility. A separate Materials Science chamber can be used for catalysts, batteries etc. studies and can also be coupled to the RIXS spectrometer.

Resonant Inelastic X-ray Scattering (RIXS) branch with very high resolving power (aim combined RP=30000) and 10m spectrometer with constant variable scattering angle over 100 degrees.

Open experimental area with the possibility of installing user chambers or using beamline instruments for example for soft x-ray diffraction or coherence experiments.
Status:  open

Disciplines

  • Physics
  • Materials and Engineering
  • Chemistry

Applications

  • Magnetism
  • Electronic Structure
  • Materials (e.g. batteries, catalysts)

Techniques

  • REXS - Resonant Elastic X-ray Scattering
  • RIXS - Resonant Inelastic X-ray Scattering
  • RXES - Resonant X-ray Emission Spectroscopy
  • XAS - X-ray Absorption Spectroscopy
  • XANES - X-ray Absorption Near Edge Structure
  • XLD - X-ray Linear Dichroism
  • XMCD - X-ray Magnetic Circular Dichroism
  • XMLD - X-ray Magnetic Linear Dichroism

Energy range

  • 0.4 - 1.6  keV

Beam size

  • Minimum (H x V) : 10.0 x 2.0  µm²
  • Maximum (H x V) : 2.0 x 2.0  mm²

Sample environments

  • XMCD:
  • 9T high magnetic field along the beam direction - split coil
  • 4T high magnetic field perpendicular to the beam direction
  • UHV sample environment - 10-10mbar range
  • Sample temperature 6-300K
  • Fast sweeping (4-8T/minute)
  • RIXS:
  • sample goniometer
  • sample temperature ~20-300K
  • scattering angles 149.5 (back scattering) -50 (forward scattering) degrees

Detectors

  • XMCD Branch:
  • Total electron yield - drain current measurement
  • Total fluorescence yield - photodiode
  • Partial fluorescence yield - RIXS detector
  • RIXS detector arm - CMOS camera
  • RIXS Branch:
  • Total electron yield - drain current measurement
  • Total fluorescence yield - photodiode
  • RIXS detector arm - CCD camera

The beamline ID32 at the ESRF for soft X-ray high energy resolution resonant inelastic X-ray scattering and polarization dependent X-ray absorption spectroscopy
N.B. Brookes, F. Yakhou-Harris, K. Kummer, A. Fondacaro, J.C. Cezar,D. Betto, E. Velez-Fort, A. Amorese, G. Ghiringhelli, L. Braicovich, R. Barrett, G. Berruyer, F.Cianciosi, L. Eybert, P. Marion, P. van der Linden, L. Zhang
Nucl. Instrum. Methods A 903, 175 (2018).

https://doi.org/10.1016/j.nima.2018.07.001