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ID32 - Soft X-ray spectroscopy
Synopsis
X-ray Magnetic Circular Dichroism (XMCD) branch with high field superconducting magnet, variable X-ray spot size at the sample, coupled to a RIXS spectrometer and surface science preparation facility. A separate Materials Science chamber can be used for catalysts, batteries etc. studies and can also be coupled to the RIXS spectrometer.Resonant Inelastic X-ray Scattering (RIXS) branch with very high resolving power (aim combined RP=30000) and 10m spectrometer with constant variable scattering angle over 100 degrees.
Open experimental area with the possibility of installing user chambers or using beamline instruments for example for soft x-ray diffraction or coherence experiments.
Status:
open
Disciplines
- Physics
- Materials and Engineering
- Chemistry
Applications
- Magnetism
- Electronic Structure
- Materials (e.g. batteries, catalysts)
Techniques
- REXS - Resonant Elastic X-ray Scattering
- RIXS - Resonant Inelastic X-ray Scattering
- RXES - Resonant X-ray Emission Spectroscopy
- XAS - X-ray Absorption Spectroscopy
- XANES - X-ray Absorption Near Edge Structure
- XLD - X-ray Linear Dichroism
- XMCD - X-ray Magnetic Circular Dichroism
- XMLD - X-ray Magnetic Linear Dichroism
Energy range
- 0.4 - 1.6 keV
Beam size
- Minimum (H x V) : 10.0 x 2.0 µm²
- Maximum (H x V) : 2.0 x 2.0 mm²
Sample environments
- XMCD:
- 9T high magnetic field along the beam direction - split coil
- 4T high magnetic field perpendicular to the beam direction
- UHV sample environment - 10-10mbar range
- Sample temperature 6-300K
- Fast sweeping (4-8T/minute)
- RIXS:
- sample goniometer
- sample temperature ~20-300K
- scattering angles 149.5 (back scattering) -50 (forward scattering) degrees
Detectors
- XMCD Branch:
- Total electron yield - drain current measurement
- Total fluorescence yield - photodiode
- Partial fluorescence yield - RIXS detector
- RIXS detector arm - CMOS camera
- RIXS Branch:
- Total electron yield - drain current measurement
- Total fluorescence yield - photodiode
- RIXS detector arm - CCD camera
The beamline ID32 at the ESRF for soft X-ray high energy resolution resonant inelastic X-ray scattering and polarization dependent X-ray absorption spectroscopy
N.B. Brookes, F. Yakhou-Harris, K. Kummer, A. Fondacaro, J.C. Cezar,D. Betto, E. Velez-Fort, A. Amorese, G. Ghiringhelli, L. Braicovich, R. Barrett, G. Berruyer, F.Cianciosi, L. Eybert, P. Marion, P. van der Linden, L. Zhang
Nucl. Instrum. Methods A 903, 175 (2018).
https://doi.org/10.1016/j.nima.2018.07.001



