Synopsis
ID13 is dedicated to high-spatial-resolution diffraction and scattering experiments using focused monochromatic x-ray beams. Two endstations, a microbranch and a nanobranch, are operated in serial mode.
Status:
open
Disciplines
- Life Sciences
- Materials and Engineering
- Environmental Sciences
- Earth and Planetary Sciences
- Chemistry
- Physics
- Cultural Heritage
- Medicine
Applications
- Hierarchically structured materials
- Biological fibers and tissues (bio-materials, bio-medical applications)
- Polymer research
- Food science
- Earth and planetary science
- Nano-composites
- Semiconductors
- Nano-structures
- Nanobeam x-ray optics
Techniques
-
MicroXRF - micro X-ray fluorescence
-
Microbeam
-
Microcrystallography
-
Ptychography
-
SAXS - small-angle X-ray scattering
-
XRD - X-ray diffraction
Beam size
- Minimum (H x V) : 100.0
x 100.0
nm²
-
Maximum (H x V) : 20.0
x 20.0
µm²
Sample environments
- Humdidity control for small samples (< 1 mm^3)
- Nano-Calorimetry
- Micro-fluidics
- Low temperature (90K, liquid-nitrogen-based cryostream, microbranch only)
Detectors
- Dectris EigerX 4M (2070 x 2167 pixel, 75 micron pixel size)
- Maxipix 2x2 four-element pixel detector (516 x 516 pixel, 55 micron pixel size)
- 2 VortexEM XRF detectors (on permanent loan from Ghent University)
Technical details
The available beam parameters such as spot size, divergence, and flux vary with the incident photon energy (e.g. highest flux available close to standard energies 13 keV). In SAXS with nanobeam scanning, minimum q is coupled with beam size. Various combinations of scanning mode, beam size, and fluorescence mode are available depending on the technique chosen.
Investigation of the microstructure of a graded ZrN/Ti0.33Al0.67N multilayer coating using cross-sectional characterization methods
Frank F., Tkadletz M., Saringer C., Czettl C., Pohler M., Burghammer M., Todt J., Zalesak J., Keckes J., Schalk N.,
Surface & Coatings Technology 453, 129126-1-129126-8 (2023)
Lead(II) formate in Rembrandt’s night watch: Detection and distribution from the macro‐ to the micro‐scale
Gonzalez V., Fazlic I., Cotte M., Vanmeert F., De Meyer S., Hermans J., van Loon A., Janssens K., Noble P., Keune K.,
Angewandte Chemie International Edition , epub (2023)
Bone mineral properties and 3D orientation of human lamellar bone around cement lines and the Haversian system
Grünewald T.A., Wittig N.K., Johannes A., Palle J., Rack A., Burghammer M., Birkedal H.,
IUCrJ 10, 189-198 (2023)
Variation in the hierarchical structure of lignin-blended cellulose precursor fibers
Liu J., Bengtsson J., Yu S., Burghammer M., Jedvert K.,
International Journal of Biological Macromolecules 225, 1555-1561 (2023)
Ultrathin positively charged electrode skin for durable anion-intercalation battery chemistries
Sabaghi D., Wang Z., Bhauriyal P., Lu Q., Morag A., Mikhailovia D., Hashemi P., Li D., Neumann C., Liao Z., Dominic A.M., Nia A.S., Dong R., Zschech E., Turchanin A., Heine T., Yu M., Feng X.,
Nature Communications 14, 760-1-760-11 (2023)
Wnt/β-catenin signaling induces axial elasticity patterns of Hydra extracellular matrix
Veschgini M., Suzuki R., Kling S., Petersen H.O., Bergheim B.G., Abuillan W., Linke P., Kaufmann S., Burghammer M., Engel U., Stein F., Özbek S., Holstein T.W., Tanaka M.,
iScience 26, 106416-1-106416-23 (2023)
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