• portable powder–liquid high-corrosion-resistant reaction cell
  • Powder reactants and/or products are kept at a fixed position in a vertical geometry in the X-ray pathway by a porous membrane, under forced liquid reflux circulation
  • X-ray powder diffraction (XRD)
  • X-ray absorption spectroscopy (XAS)

 

         Powder cell.png

 

P. Ferrer, I. da Silva, J. Rubio-Zuazo, B. F. Alfonso, C. Trobajo, S. Khainakov, J. R. Garcia, S. Garcia-Granda, G. R. Castro. “A flow-through reaction cell for in situ X-ray diffraction and absorption studies of heterogeneous powder-liquid reactions and phase transformations” Journal of synchrotron radiation, 19 (2012) pp. 93-100
https://doi.org/10.1107/s0909049511040374

P Ferrer, I da Silva, C Heyman, J Rubio-Zuazo and G R Castro “A portable powder-liquid high corrosion-resistant reaction cell for in situ X-ray diffraction and absorption studies of heterogeneous powder-liquid reactions and phase transformations”, Journal of Physics: Conference Series. 425 132001 (2013).
https://doi.org/10.1088/1742-6596/425/13/132001