The ID21 beamline is dedicated to micro and nano-X ray spectroscopy, 2D X-ray fluorescence (XRF) mapping and X-ray absorption spectroscopy (XAS), in the tender X-ray domain (2.1-10.5keV). These two techniques can be combined to acquire multi-energy XRF maps. Therefore, this beamline offers 2D elemental mapping and speciation information (in 0D, 1D and 2D), and is particularly optimized for the detection and chemical analysis of elements from P to Zn. Heavier elements can be analyzed through their L and M absorption edges.
The beamline has recently been refurbished, and offers now two scanning X-ray microscopes: a new nanoscope (nano-SXM), optimized for high speed, high resolution (<180nm) nano-XRF mapping, and for nano-XAS, which complements and outperforms the "old" microscope, which has been preserved with the study of larger samples, with micrometric and submillimetric beam. Both microscopes are operated under vacuum, either at room temperature or in cryogenics conditions.
Status:
open
Disciplines
Medicine
Cultural Heritage
Environmental Sciences
Earth and Planetary Sciences
Materials and Engineering
Physics
Life Sciences
Chemistry
Applications
Cultural Heritage (e.g. paintings, ceramics, glasses)
M. Cotte, E. Pouyet, M. Salomé, C. Rivard, W. De Nolf, H. Castillo-Michel, T. Fabris, L. Monico, K. Janssens, T. Wang, P. Sciau, L. Verger, L. Cormier, O. Dargaud, E. Brun, D. Bugnazet, B. Fayard, B. Hesse, A. E. Pradas del Real, G. Veronesi, J. Langlois, N. Balcar, Y. Vandenberghe, V. A. Solé, J. Kieffer, R. Barrett, C. Cohen, C. Cornu, R. Baker, E. Gagliardini, E. Papillon and J. Susini, "The ID21 X-ray and infrared microscopy beamline at the ESRF: status and recent applications to artistic materials." Journal of Analytical Atomic Spectrometry (2017). http://pubs.rsc.org/-/content/articlehtml/2016/ja/c6ja00356g
M. Salomé, M. Cotte, R. Baker, R. Barrett, N. Benseny-Cases, G. Berruyer, D. Bugnazet, H. Castillo-Michel, C. Cornu, B. Fayard, E. Gagliardini, R. Hino, J. Morse, E. Papillon, E. Pouyet, C. Rivard, V. A. Solé, J. Susini and G. Veronesi, "The ID21 Scanning X-ray Microscope at ESRF", Journal of Physics: Conference Series, 425, 182004 (2013). http://dx.doi.org/10.1088/1742-6596/425/18/182004
Costantino C., Monico L., Rosi F., Vivani R., Romani A., Colocho Hurtarte L.C., Villalobos-Portillo E., Sahle C.J., Huthwelker T., Dejoie C., Burghammer M., Cotte M.,
Applied Spectroscopy , epub (2024)
Gonzalez-Rivas M.U., Aamlid S.S., Rutherford M.R., Freese J., Sutarto R., Chen N., Villalobos-Portillo E.E., Castillo-Michel H., Kim M., Takagi H., Green R.J., Hallas A.M.,
Journal of the American Chemical Society 146, 26048-26059 (2024)
Haukelidsaeter S., Boersma A.S., Piso L., Lenstra W.K., van Helmond N.A.G.M., Schoonenberg F., van der Pol E., Hurtarte L.C.C., van der Wielen P.W.J.J., Behrends T., van Kessel M.A.H.J., Lücker S., Slomp C.P.,
Applied Geochemistry 162, 105904-1-105904-12 (2024)
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