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BM01

Synopsis

BM01 offers a variety of synchrotron diffraction tools (powder, single crystal, and grazing-incidence surface diffraction, high-resolution reciprocal space mapping, small-angle scattering and combinatorial use of several techniques), mostly focused on the in-situ and operando diffraction experiments in the field of energy-related materials and processes.
Status:  open

Disciplines

  • Environmental Sciences
  • Chemistry
  • Materials and Engineering
  • Physics
  • Life Sciences

Applications

  • Energy
  • Solid state physics and chemistry
  • Advanced materials
  • In-situ and operando crystallography

Techniques

  • GISAXS - Grazing Incidence Small Angle X-ray Scattering
  • GIXRD - Grazing Incidence X-ray Diffraction
  • HP-XRD - High-Pressure X-ray Diffraction
  • HT-XRD - High-Temperature X-ray Diffraction
  • SAXS - Small-Angle X-ray Scattering
  • SCXRD - Single Crystal X-ray Diffraction, SC-XRD, SCD, SXRD
  • WAXS - Wide-angle X-ray Scattering
  • XDS - X-ray Diffuse Scattering
  • XRD - X-ray Diffraction
  • XRPD - X-ray Powder Diffraction
  • XRR - X-ray Reflectometry, X-ray reflectivity, X-ray specular reflectivity

Energy range

  • 12.0 - 25.0  keV

Beam size

  • Minimum (H x V) : 160.0 x 80.0  µm²
  • Maximum (H x V) : 500.0 x 300.0  µm²

Sample environments

  • Electrochemical cells
    Electrolyzer cells
    Low temperatures: CryoVac 2-300K
    High temperatures: locally developed heaters, from 22C to 1500C
    Hydrostatic pressure: 1-1000 bars
    Gas pressure system: 0-40 bars
    Electric field: 0-1 kV, for single crystals and thin films
    5-cells battery operando rig, gas loading manifold

Detectors

  • Dectris Pilatus 2M (WAXS)
    Dectris Pilatus 2M (SAXS)