Publications

[2025 | 2024 | 2023 | 2022 | 2021 | 2020 | 2019 | 2018 | 2017 | 2016  | 2015]

2025

Lee, S.; Pilipchuk, M.; Yildirim, C.; Greeley, D.; Shi, Q.; Berman, T. D.; Creuziger, A.; Rust, E.; Detlefs, C.; Sundararaghavan, V.; Allison, J. E.; Bucsek, A. (2025).
Three-dimensional nucleation and growth of deformation twins in magnesium
Science 389, 632.
DOI: 10.1126/science.adv3460

Detlefs, C.; Henningsson, A.; Kanesalingam, B.; Cretton, A. A. W.; Corley-Wiciak, C.; Frankus, F. T.; Pal, D.; Irvine, S.; Borgi, S.; Poulsen, H. F.; Yildirim, C.; Dresselhaus-Marais L. E. (2025).
Oblique diffraction geometry for the observation of several non-coplanar Bragg reflections under identical illumination
J. Appl. Cryst. 58, 1439.
DOI: 10.1107/S1600576725005862

Zelenika, A.; Cretton, A. A. W.; Frankus, F.; Borgi, S.; Grumsen, F. B.; Yildirim, C.; Detlefs, C.; Winther, G.; Poulsen, H. F. (2025).
Observing formation and evolution of dislocation cells during plastic deformation
Scientific Reports 15, 8655.
DOI: 10.1038/s41598-025-88262-3

Ziegelwanger, T.; Reisinger, M.; Petersmann, M.; Van Petegem, S.; Rodriguez-Lamas, R.; Todt, J.; Meindlhumer, M; Keckes, J.; Yildirim, C. (2025).
Intragranular strain and mosaicity in Cu thin films during fast thermomechanical fatigue
npj Materials Degradation 9, 79.
10.1038/s41529-025-00629-z

Cretton, A. A. W.; Zelenika, A.; Frankus, F.; Yıldırım, C.; Detlefs, C.; Grumsen, F. B.; Winther, G.; Poulsen, H. F. (2025).
Observation of the formation and sharpening of geometrically necessary boundaries
Materials Research Letters13 , 759.
10.1080/21663831.2025.2511893

Isern, H.; Brochard, T.; Dufrane, T.; Brumund, P.; Papillon, E.; Scortani, D.; Hino, R.; Yildirim, C.; Rodriguez Lamas, R.; Li, Y.; Sarkis M.; Detlefs, C. (2025).
The ESRF dark-field x-ray microscope at ID03
J. Phys. Conf. Ser. 3010, 012163.
10.1088/1742-6596/3010/1/012163

2024

Yildirim C.; Flatscher F.; Ganschow S.; Lassnig A.; Gammer C.; Todt J.; Keckes J.; Rettenwander D. (2024).
Understanding the origin of lithium dendrite branching in Li_6.5La₃Zr_1.5Ta_0.5O₁₂ solid-state electrolyte via microscopy measurements
Nature Commun. 15, 8207.
10.1038/s41467-024-52412-4

Oliveira L.; Zhang M.; Koruza J.; Rodiquez-Lamas R.; Yildirim C.; Simons H. (2024)
Heterogeneous Antiferroelectric Ordering in NaNbO₃–SrSnO₃ Ceramics Revealed by Direct Superstructure Imaging
ACS Materials Lett. 6, 3745.
10.1021/acsmaterialslett.4c01080

Oliveira L.; Zhang M.; Höfling M.; Rodriguez-Lamas R.; Yildirim C.; Koruza J.; Simons H. (2024)
Coupled local residual shear and compressive strain in NaNbO₃ ceramics under cooling
Acta Mater. 266, 119640.
10.1016/j.actamat.2023.119640

Zelenika A.; Yildirim C.; Detlefs C.; Rodriguez-Lamas r.; Grumsen F.; Poulsen H.; Winther G. (2024)
3D microstructural and strain evolution during the early stages of tensile deformation
Acta Mater. 270, 119838.
10.1016/j.actamat.2024.119838

Borgi S.; Raeder T.; Carlsen M.; Detlefs C.; Winther G.; Poulsen H.(2024)
Simulations of dislocation contrast in dark-field X-ray microscopy
Journal of Applied Crystallography 57, 358.
10.1107/s1600576724001183

Lee S.; Berman T.; Yildirim C.; Detlefs C.; Allison J.; Bucsek A.(2024)
Multiscale in-situ characterization of static recrystallization using dark-field X-ray microscopy and high-resolution X-ray diffraction
Scientific Reports 14, 6241.
10.1038/s41598-024-56546-9

 

2023

Yildirim C.; Poulsen H.; Winther G.; Detlefs C.; Huang P.; Dresselhaus-Marais L.(2023)
Extensive 3D mapping of dislocation structures in bulk aluminum
Scientific Reports 13, 3834.
10.1038/s41598-023-30767-w

Garriga Ferrer J.; Rodriguez Lamas R.; Payno H.; de Nolf W.; Cook P.; Sole Jover V.; Yildirim C.; Detlefs C.(2023)
darfix - data analysis for dark-field X-ray microscopy
J. of Synchrotron Radiation 30, 527.
10.1107/s1600577523001674

Hlushko K.; Ziegelwanger T.; Reisinger M.; Todt J.; Meindlhumer M.; Beuer S.; Rommel M.; Greving I.; Flenner S.; Kopeček J.; Keckes J.; Detlefs C.(2023)
Intragranular thermal fatigue of Cu thin films: Near-grain boundary hardening, strain localization and voiding
Acta Mater. 253, 118961.
10.1016/j.actamat.2023.118961

Chen Y.; Tang Y.; Collins D.; Clark S.; Ludwig W.; Rodriguez-Lamas R.; Detlefs C.; Reed R.; Lee P.; Withers P.; Yildirim C.(2023)
High-resolution 3D strain and orientation mapping within a grain of a directed energy deposition laser additively manufactured superalloy
Scripta Materialia 234, 115579.
10.1016/j.scriptamat.2023.115579

Wehbe M.; Charles M.; Baril K.; Alloing B.; Pino Munoz D.; Labchir N.; Zuniga-Perez J.; Detlefs C.; Yildirim C.; Gergaud P.(2023)
Study of GaN coalescence by dark-field X-ray microscopy at the nanoscale
Journal of Applied Crystallography 56, 343.
10.1107/s160057672300287x

Gustafson S.; Ludwig W.; Rodriguez-Lamas R.; Yildirim C.; Shanks K.; Detlefs C.; Sangid M.; Gergaud P.(2023)
Revealing 3D intragranular micromechanical fields at triple junctions
Acta Materialia 260, 119300.
10.1016/j.actamat.2023.119300

 

2022

Yildirim C.; Mavrikakis N.; Cook P.; Rodriguez-Lamas R.; Kutsal M.; Poulsen H.; Detlefs C.(2022)
4D microstructural evolution in a heavily deformed ferritic alloy: A new perspective in recrystallisation studies
Scripta Materialia 214, 114689.
10.1016/j.scriptamat.2022.114689

Kutsal M.; Poulsen H.; Winther G.; Sorensen H.; Detlefs C.(2022)
High-resolution 3D X-ray diffraction microscopy: 3D mapping of deformed metal microstructures
J. of Applied Crystallography 55, 1125.
10.1107/s1600576722007361

Celestre R.; Antipov S.; Gomez E.; Zinn T.; Barrett R.; Roth T.(2022)
Polished diamond X-ray lenses
J. of Synchrotron Radiation 29, 629.
10.1107/s1600577522001795

Carlsen M.; Raeder T.; Yildirim C.; Rodriguez-Lamas R.; Detlefs C.; Simons H.(2022)
Fourier ptychographic dark field x-ray microscopy
Optics Express 30, 2949.
10.1364/oe.447657

Schoeppler V.; Cook P.; Detlefs C.; Demichelis R.; Zlotnikov I.(2022)
Untangling the Mechanisms of Lattice Distortions in Biogenic Crystals across Scales
Advanced Materials 34, 2200690.
10.1002/adma.202200690

Yildirim C.; Mavrikakis N.; Cook P.; Rodriguez Lamas R.; Poulsen H.; Detlefs C.; Kutsal M.(2022)
Multiscale Exploration of Texture and Microstructure Development in Recrystallization Annealing of Heavily Deformed Ferritic Alloys
Mater. Sci. Eng.1249 , 012044.
110.1088/1757-899x/1249/1/012044

Carlsen M.; Detlefs C.; Yildirim C.; Raeder T.; Simons H.(2022)
Simulating dark-field X-ray microscopy images with wavefront propagation techniques
Acta Cryst. A78, 482.
10.1107/s205327332200866x

2021

Porz L.; Klomp A.; Fang X.; Li N.; Yildirim C.; Detlefs C.; Bruder E.; Homfling M.; Rheinheimer W.; Patterson E.; Gao P.; Durst K.; Nakamura A.; Albe K.; Simons H.; Roedel J. (2021)
Dislocation-toughened ceramics
Matter. Horiz. 8,1528.
10.1039/d0mh02033h

Dresselhaus-Marais L.; Winther G.; Howard M.; Gonzalez A.; Breckling S.; Yildirim C.; Cook P.; Kutsal M.; Simons H.; Detlefs C.; Eggert J.; Poulsen H.(2021) In situ visualization of long-range defect interactions at the edge of melting Sci. Adv. 7,8311.10.1126/sciadv.abe8311

Yildirim C.; Jessop C.; Ahlstrom J.; Detlefs C.; Zhang Y.(2021) 3D mapping of orientation variation and local residual stress within individual grains of pearlitic steel using synchrotron dark field X-ray microscopy J. of Applied Crystallography197,113783.10.1016/j.scriptamat.2021.113783

Poulsen H.; Dresselhaus-Marais L.; Carlsen M.; Detlefs C.; Winther G.(2021) Geometrical-optics formalism to model contrast in dark-field X-ray microscopy Scripta Materialia 54,1555.10.1016/j.scriptamat.2021.113783

Schultheiss; J.; Porz L.; Kodumudi Venkataraman L.; Hoefling M.; Yildirim C.; Cook P.; Detlefs C.; Gorfman S.; Roedel J.; Simons H.(2021) Rocking Curve Imaging Investigation of the Long-Range Distortion Field between Parallel Dislocations with Opposite Burgers Vectors Applied Science 11, 9054 10.1016/j.scriptamat.2021.113878

Caliste T.; Drouin A.; Caliste D.; Detlefs C.; Baruchel J.(2021) Quantitative mapping of nanotwin variants in the bulk Applied Sciences 199, 10.3390/app11199054

Snigireva I.; Polikarpov M.; Snigirev A. (2021). Diamond X-Ray Refractive Optics, Synchrotron Rad. News, 34, 12-20. 10.1080/08940886.2021.2022387

Ormstrup J., Østergaard, E., Christensen, M., Yildirim, C., Cook, P., Kutsal, M., Olsen, T., Simons, H. (2021)  Bulk heterogeneity in barium titanate above the Curie temperature, Appl. Phys. Lett 119, 202901 10.1080/08940886.2021.2022387

 

2020

Ahl S.R., Simons H., Detlefs C., Jensen D.J., Poulsen H.F. (2020). Subgrain dynamics during recovery of partly recrystallized aluminum Acta Materialia 185, 142-148. http://dx.doi.org/10.1016/j.actamat.2019.10.042

Gustafson S., Ludwig W., Shade P., Naragani D., Pagan D., Cook P., Yildirim C., Detlefs C., Sangid M.D. (2020). Quantifying microscale drivers for fatigue failure via coupled synchrotron X-ray characterization and simulations Nature Communications 11, 3189-1-3189-10. http://dx.doi.org/10.1038/s41467-020-16894-2

Hlushko K., Keckes J., Ressel G., Pörnbacher J., Ecker W., Kutsal M., Cook P.K., Detlefs C., Yildirim C. (2020). Dark-field X-ray microscopy reveals mosaicity and strain gradients across sub-surface TiC and TiN particles in steel matrix composites Scripta Materialia 187, 402-406. http://dx.doi.org/10.1016/j.scriptamat.2020.06.053

Ormstrup J., Ostergaard E.V., Detlefs C., Mathiesen R.H., Yildirim C., Kutsal M., Cook P.K., Watier Y., Cosculluela C., Simons H. (2020). Imaging microstructural dynamics and strain fields in electro-active materials in situ with dark field x-ray microscopy Review of Scientific Instruments 91, 065103-1-065103-8. https://doi.org/10.1063/1.5142319

Yildirim C., Vitoux H., Dresselhaus-Marais L.E., Steinmann R., Watier Y., Cook P.K., Kutsal M., Detlefs C. (2020). Radiation furnace for synchrotron dark-field x-ray microscopy experiments Review of Scientific Instruments 91, 065109-1-065109-8. https://doi.org/10.1063/1.5141139

 

2019

Sierra, J. X., Poulsen, H. F., Jørgensen, P. S., Detlefs, C., Cook, P., Simons, H., … Bowen, J. R. (2019). In-operando observation of microstructural evolution in a solid oxide cell electrolyte operating at high polarization. Journal of Power Sources, 413, 351–359. https://doi.org/10.1016/j.jpowsour.2018.12.057

Kutsal, M., Bernard, P., Berruyer, G., Cook, P. K., Hino, R., Jakobsen, A. C., … Detlefs, C. (2019). The ESRF dark-field x-ray microscope at ID06. IOP Conference Series: Materials Science and Engineering, 580, 012007. https://doi.org/10.1088/1757-899X/580/1/012007

Mavrikakis, N., Detlefs, C., Cook, P. K., Kutsal, M., Campos, A. P. C., Gauvin, M., … Yildirim, C. (2019). A multi-scale study of the interaction of Sn solutes with dislocations during static recovery in α-Fe. Acta Materialia, 174, 92–104. https://doi.org/10.1016/j.actamat.2019.05.021

Murray, K. T., Pedersen, A. F., Mohacsi, I., Detlefs, C., Morgan, A. J., Prasciolu, M., … Bajt, S. (2019). Multilayer Laue lenses at high X-ray energies: performance and applications. Optics Express, 27(5), 7120. https://doi.org/10.1364/OE.27.007120

Falch, K. V., Detlefs, C., Christensen, M. S., Paganin, D., & Mathiesen, R. (2019). Experimental investigation of Gaussian random phase screen model for x-ray diffusers. Optics Express, 27(15), 20311. https://doi.org/10.1364/OE.27.020311

Jakobsen, A. C., Simons, H., Ludwig, W., Yildirim, C., Leemreize, H., Porz, L., … Poulsen, H. F. (2019). Mapping of individual dislocations with dark-field X-ray microscopy. Journal of Applied Crystallography, 52. https://doi.org/10.1107/S1600576718017302

Simons, H., Jakobsen, A. C., Ahl, S. R., Poulsen, H. F., Pantleon, W., Chu, Y.-H., … Valanoor, N. (2019). Nondestructive Mapping of Long-Range Dislocation Strain Fields in an Epitaxial Complex Metal Oxide. Nano Letters, 19(3), 1445–1450. https://doi.org/10.1021/acs.nanolett.8b03839

 

2018

 

Simons, H., Haugen, A. B., Jakobsen, A. C., Schmidt, S., Stöhr, F., Majkut, M., … Poulsen, H. F. (2018). Long-range symmetry breaking in embedded ferroelectrics. Nature Materials, 17(9). https://doi.org/10.1038/s41563-018-0116-3

 

Poulsen, H. F., Cook, P. K., Leemreize, H., Pedersen, A. F., Yildirim, C., Kutsal, M., … Detlefs, C. (2018). Reciprocal space mapping and strain scanning using X-ray diffraction microscopy. Journal of Applied Crystallography, 51(5), 1428–1436. https://doi.org/10.1107/S1600576718011378

 

Falch, K. V., Detlefs, C., Snigirev, A., & Mathiesen, R. H. (2018). Analytical transmission cross-coefficients for pink beam X-ray microscopy based on compound refractive lenses. Ultramicroscopy, 184, 1–7. https://doi.org/10.1016/j.ultramic.2017.09.010

 

Falch, K. V., Lyubomirsky, M., Casari, D., Snigirev, A., Snigireva, I., Detlefs, C., … Mathiesen, R. H. (2018). Zernike phase contrast in high-energy x-ray transmission microscopy based on refractive optics. Ultramicroscopy, 184, 267–273. https://doi.org/10.1016/j.ultramic.2017.10.001

 

Cook, P. K., Simons, H., Jakobsen, A. C., Yildirim, C., Poulsen, H. F., & Detlefs, C. (2018). Insights into the Exceptional Crystallographic Order of Biominerals Using Dark-Field X-ray Microscopy. Microscopy and Microanalysis, 24(S2), 90–91. https://doi.org/10.1017/S1431927618012837

 

2017

 

Simons, H., Ahl, S. R., Poulsen, H. F., & Detlefs, C. (2017). Simulating and optimizing compound refractive lens-based X-ray microscopes. Journal of Synchrotron Radiation, 24(2), 392–401. https://doi.org/10.1107/S160057751602049X

 

Poulsen, H. F., Jakobsen, A. C., Simons, H., Ahl, S. R., Cook, P. K., & Detlefs, C. (2017). X-ray diffraction microscopy based on refractive optics. Journal of Applied Crystallography, 50(5), 1441–1456. https://doi.org/10.1107/S1600576717011037

 

Ahl, S. R., Simons, H., Zhang, Y. B., Detlefs, C., Stöhr, F., Jakobsen, A. C., … Poulsen, H. F. (2017). Ultra-low-angle boundary networks within recrystallizing grains. Scripta Materialia, 139. https://doi.org/10.1016/j.scriptamat.2017.06.016

 

Falch, K. V., Casari, D., Di Michiel, M., Detlefs, C., Snigireva, A., Snigireva, I., … Mathiesen, R. H. (2017). In situ hard X-ray transmission microscopy for material science. Journal of Materials Science, 52(6), 3497–3507. https://doi.org/10.1007/s10853-016-0643-8

 

Zverev, D., Barannikov, A., Snigireva, I., & Snigirev, A. (2017). X-ray refractive parabolic axicon lens. Optics Express, 25(23), 28469. https://doi.org/10.1364/OE.25.028469

 

Tran Thi, T. N., Morse, J., Caliste, D., Fernandez, B., Eon, D., Härtwig, J., … Baruchel, J. (2017). Synchrotron Bragg diffraction imaging characterization of synthetic diamond crystals for optical and electronic power device applications. Journal of Applied Crystallography, 50(2), 561–569. https://doi.org/10.1107/S1600576717003831

 

2016

 

Falch, K. V., Detlefs, C., Di Michiel, M., Snigireva, I., Snigirev, A., & Mathiesen, R. H. (2016). Correcting lateral chromatic aberrations in non-monochromatic X-ray microscopy. Applied Physics Letters, 109(5), 054103. https://doi.org/10.1063/1.4960193

 

Simons, H., Jakobsen, A. C., Ahl, S. R., Detlefs, C., & Poulsen, H. F. (2016). Multiscale 3D characterization with dark-field x-ray microscopy. MRS Bulletin, 41(6), 454–459. https://doi.org/10.1557/mrs.2016.114

 

2015

 

Simons, H., King, A., Ludwig, W., Detlefs, C., Pantleon, W., Schmidt, S., … Poulsen, H. F. (2015). Dark-field X-ray microscopy for multiscale structural characterization. Nature Communications, 6(1), 6098. https://doi.org/10.1038/ncomms7098

 

Roth, T., Detlefs, C., Snigireva, I., & Snigirev, A. (2015). X-ray diffraction microscopy based on refractive optics. Optics Communications, 340, 33–38. https://doi.org/10.1016/j.optcom.2014.11.094